Synthesis and characterization of polyaniline–camphorsulphonic acid nanotube film

Ayad, Mohamad M. and Prastomo, Niki and Matsuda, Atsunori (2010) Synthesis and characterization of polyaniline–camphorsulphonic acid nanotube film. Materials Letters, 64 (3). pp. 379-382. ISSN 0167-577X

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Abstract

Polyaniline (PANI) nanotubes were prepared in the bulk solution and as films using the aniline oxidation with ammonium peroxydisulfate in aqueous solutions of camphorsulfonic acid (CSA). The in situ PANI films produced during the oxidation of aniline in CSA and also in hydrochloric acid solutions were followed by monitoring the frequency changes of quartz crystal microbalance (QCM). The kinetics of the film formation were discussed. The scanning electron microscopy (SEM) and scanning transmission electron microscopy (STEM) showed PANI nanotubes. In addition, nanorods and nanoflowers composed from nanofibers and nanoflakes are also present to some extent. The nanotubes were characterized using UV–Vis spectroscopy.

Item Type: Article
Keywords: Polyaniline nanotube film; Camphorsulfonic acid; Quartz crystal microbalance
Subjects: 500 Science and Mathematic > 500 Science > 507 Education, Research, Related Topics
Divisions: Faculty of Engineering & Informatics > Engineering Physics
Depositing User: Administrator UMN Library
Date Deposited: 09 Dec 2021 16:54
Last Modified: 09 Dec 2021 16:54
URI: https://kc.umn.ac.id/id/eprint/19443

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